2-甲基-3-丁炔-2-醇合成路线 （共 621 条）
反应条件
1: With copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 3 h; Heating; 2: With potassium hydroxide in isopropyl alcohol 7 h; Heating; Further stages.;
参考文献
Gallardo, Hugo; Cristiano, Rodrigo; Vieira, Andre A.; Neves Filho, Ricardo A. W.; Srivastava, Rajendra M.
Synthesis, 2008 , # 4 p. 605 - 609
反应条件
quinoline; hydrogen; Lindlar's catalyst in Petroleum ether T=20°C; 10 h;
参考文献
Vani; Chida; Srinivasan; Chandrasekharam; Singh
Synthetic Communications, 2001 , vol. 31, # 2 p. 219 - 224
反应条件
hydrogen; palladium-copper; silica gel in ethanol T=25°C; P=760 Torr; Kinetics;
参考文献
Spee; Boersma; Meijer; Slagt; Van Koten; Geus
Journal of Organic Chemistry, 2001 , vol. 66, # 5 p. 1647 - 1656
反应条件
hydrogen; pentacyanocobaltate(II)(3-) in water T=45°C; P=760 Torr; 10 h; <Me2C(OH)CCH>/<Co> : 1; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Funabiki, Takuzo; Yamazaki, Yasuyuki; Sato, Yoshihiro; Yoshida, Satohiro
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 12 p. 1915 - 1918
反应条件
hydrogen in water T=45°C; P=760 Torr; 10 h; <Me2C(OH)CCH>/<Co> : 2; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 12 p. 1915 - 1918
反应条件
hydrogen; palladium-copper in water T=20°C; various catalysts, solvents, temperature; Product distributionKinetics;
参考文献
Dukhovnaya, T. M.; Dzhardamalieva, K. K.; Nigmetova, D. T.; Sokol'skii, D. V.
Russian Journal of Physical Chemistry, 1983 , vol. 57, # 3 p. 373 - 376
Zhurnal Fizicheskoi Khimii, 1983 , vol. 57, # 3 p. 617 - 620
反应条件
hydrogen; magnesium oxide; copper in ethanol T=99.9°C; P=15001.2 Torr; other catalysts (Ag/MgO, Au/MgO); Rate constantProduct distribution;
参考文献
Journal of applied chemistry of the USSR, , vol. 57, # 2 pt 2 p. 426 - 428
反应条件
P=3089.1 Torr; Hydrogenation;
参考文献
Campbell; Eby
Journal of the American Chemical Society, 1941 , vol. 63, p. 2684
反应条件
pentacyanocobaltate(II)(3-); hydrogen in water P=760 Torr; 10 h; different reagent ratio; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 12 p. 1915 - 1918
参考文献
Bayer and Co.
Patent: DE288271 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 12, p. 58
