2-甲基-3-丁炔-2-醇合成路线 （共 621 条）
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
参考文献
Murthi, Krishna K.; Salomon, Robert G.
Tetrahedron Letters, 1994 , vol. 35, # 4 p. 517 - 520
反应条件
3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide in neat (no solvent) T=70°C; 2 h; trimethylsilylation of acetylenic alcohols and glycols; solvent, reaction time and temperature, saccharine addition varied; Product distribution;
参考文献
Demina, Maria; Velikanov, Andrey; Medvedeva, Alevtina; Larina, Lyudmila; Voronkov, Mikhail
Journal of Organometallic Chemistry, 1998 , vol. 553, # 1-2 p. 129 - 133
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in dimethyl sulfoxide T=80°C; 48 h;
参考文献
Shirakawa, Eiji; Kitabata, Takaaki; Otsuka, Hidehito; Tsuchimoto, Teruhisa
Tetrahedron, 2005 , vol. 61, # 41 p. 9878 - 9885
反应条件
copper(l) iodide; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in triethylamine T=90°C; Yield given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 4 p. 1020 - 1025
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride T=70°C;
参考文献
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, , vol. 373, p. 1 - 15
反应条件
1: 1) NaH / 1) THF, heating, 2) room temperature, 1 h 2: 51 percent / BCl3 / pentane; hexane / 1 h / Ambient temperature 3: 50 percent / tetrahydrofuran; dimethylformamide View Scheme
参考文献
Bedford; Harris III; Howd; Goff; Koolpe; Petesch; Koplovitz; Sultan; Musallam
Journal of Medicinal Chemistry, 1989 , vol. 32, # 2 p. 504 - 516
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride Sonogashira coupling; Heating;
参考文献
Vasconcelos, Ursula B.; Schrader, Abel; Vilela, Guilherme D.; Borges, Antonio C.A.; Merlo, Aloir A.
Tetrahedron, 2008 , vol. 64, # 20 p. 4619 - 4626
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride T=70°C;
参考文献
Yang; Tang; Gong; Wen
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 348, p. 153 - 165
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in toluene T=65°C; Sonogashira coupling; Inert atmosphere;
参考文献
Baranov, Denis S.; Ryabichev, Aleksey A.; Mamatyuk, Victor I.; Gatilov, Yurii V.; Kartsev, Victor G.; Vasilevsky, Sergei F.
Mendeleev Communications, 2012 , vol. 22, # 2 p. 114 - 116
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine in tetrahydrofuran T=80°C; Sonogashira Cross-Coupling; 12 h; Inert atmosphere;
参考文献
Gschneidtner, Tina A.; Moth-Poulsen, Kasper
Tetrahedron Letters, 2013 , vol. 54, # 40 p. 5426 - 5429
