2-甲基-3-丁炔-2-醇合成路线 （共 621 条）
反应条件
(((3-hydroxypropyl)carbonylcyclopentadienyl)cobalt)-η4-cyclooctadiene in methanol; water
参考文献
Sigman; Fatland; Eaton
Journal of the American Chemical Society, 1998 , vol. 120, # 20 p. 5130 - 5131
反应条件
lt;Ni(NCS)(Clt;*gt;C-C(CH3)2(OH))(Ph3P)2gt; in diethylamine
6 h; Heating;
参考文献
Bicev, Peter; Furlani, Anita; Russo, Maria Vittoria
Gazzetta Chimica Italiana, 1980 , vol. 110, # 1 p. 25 - 30
反应条件
bis(acetylacetonate)nickel(II)
T=40°C; 0.666667 h;
参考文献
Ananikov; Zalesskiy; Orlov; Beletskaya
Russian Chemical Bulletin, 2006 , vol. 55, # 11 p. 2109 - 2113
反应条件
{NiBr2(Tri-{n-butyl}-phosphin)2} in hexane
5 h; Heating;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
{NiBr2(Tri-{n-butyl}-phosphin)2} in Petroleum ether
7 h; Heating;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
NiBr2(PPh3)2 in benzene
5 h; Heating;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
{NiBr2(Tri-{n-butyl}-phosphin)2} in Petroleum ether
7 h; Heating; Yields of byproduct given;
参考文献
Furlani, Anita; Hornemann, Karl Heinz; Russo, Maria Vittoria; Villa, Angiola Chiesi; Guastini, Carlo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 7 p. 429 - 436
反应条件
bis(1,5-cyclooctadiene)nickel (0); tris(4-methoxyphenyl)-phosphine in toluene
T=60 - 62°C; 5 h; var. P-ligands; Product distribution;
参考文献
Hartmann, W.; Preuss, K. D.; Singer, H.
Journal of Organometallic Chemistry, 1983 , vol. 258, # 2 p. 235 - 246
反应条件
silica gel; nickel
T=110°C; 2 h; other Ni-catalysts; Product distribution;
参考文献
Walther, Dirk; Braun, Dagmar
Zeitschrift fuer Chemie (Stuttgart, Germany), 1988 , vol. 28, # 3 p. 106 - 107
反应条件
1: water; NH4Cl; CuCl; oxygen / 0 - 5 °C
2: Raney nickel; methanol / 100 °C / 51485.6 - 80905.8 Torr / Hydrogenation
View Scheme
参考文献
Salkind; Aisikowitsch
Zhurnal Obshchei Khimii, vol. 7, p. 230
Chem. Zentralbl., 1937 , vol. 108, # I p. 4783
