2-甲基-3-丁炔-2-醇合成路线 （共 621 条）
反应条件
hydrogen; 1,4-di(diphenylphosphino)-butane; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in dichloromethane
T=95°C; P=41371.8 Torr; 36 h;
参考文献
Yu, Wing-Yiu; Alper, Howard
Journal of Organic Chemistry, 1997 , vol. 62, # 17 p. 5684 - 5687
反应条件
methanol; hydrogen iodide in hexane
T=150°C; P=76000 Torr; 6 h;
参考文献
Gusev, B. P.; El'perina, E. A.; Kucherov, V. F.; Pirozhkov, S. D.; Lapidus, A. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 3 p. 421 - 425
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 3 p. 603 - 607
反应条件
[Pd(NCCH3)2(PPh3)2](BF4)2 in tetrahydrofuran
T=50°C; P=7355.08 Torr; Yield given. Yields of byproduct given;
参考文献
Matsushita, Koichi; Komori, Tsunenori; Oi, Shuichi; Inoue, Yoshio
Tetrahedron Letters, 1994 , vol. 35, # 32 p. 5889 - 5890
反应条件
hydrogen iodide in hexane
T=150°C; P=76000 Torr; 6 h;
参考文献
Gusev, B. P.; El'perina, E. A.; Kucherov, V. F.; Pirozhkov, S. D.; Lapidus, A. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 3 p. 421 - 425
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 3 p. 603 - 607
参考文献
Jones et al.
Journal of the Chemical Society, 1957 , p. 4628,4631
Full Text Show Details
Bergmann; Zimkin
Journal of the Chemical Society, 1950 , p. 3455
反应条件
[rhenium(I)pentacarbonyl(chloride)] in hexane
T=60°C; 24 h;
参考文献
Zeng, Hanxiang; Ju, Jia; Hua, Ruimao
Tetrahedron Letters, 2011 , vol. 52, # 30 p. 3926 - 3928
反应条件
1: 2-methyl-but-3-yn-2-ol With n-butyllithium in tetrahydrofuran; hexane
T=-30°C; 1 h;
2: cyclopentanone in tetrahydrofuran; hexane
T=-30 - 20°C;
参考文献
Koval'skaya; Kozlov; Dikusar
Russian Journal of General Chemistry, 2004 , vol. 74, # 6 p. 897 - 902
反应条件
diethyl ether
anschliessend Behandeln mit Cyclopentanon;
参考文献
Salkind; Gwerdziteli
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 855,861
Chem. Zentralbl., 1939 , vol. 110, # II p. 3803
反应条件
1: mercury boron fluoride; trichloroacetic acid / 20 - 25 °C
2: KHSO4 / Destillation
View Scheme
参考文献
Nasarow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1940 , p. 219
Chem.Abstr., 1942 , p. 746
反应条件
in N,N-dimethyl-formamide
electrolyses;
参考文献
Dapremont, Christine; Cals, Patrick; Commeyras, A.; Amatore, Christian
Journal of Fluorine Chemistry, 1992 , vol. 56, # 2 p. 249 - 258
