N-(4-甲氧基苯基)-4-甲基苯磺酰胺合成路线 （共 18 条）
反应条件
1: 45 percent / copper bronze, K2CO3 / 4 h / Heating 2: 73 percent / ethanol / 7 h / Irradiation View Scheme
参考文献
Hall, Robin J.; Marchant, Jeremy; Oliveira-Campos, Ana M. F.; Queiroz, Maria-Joao R. P.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3439 - 3450
反应条件
titanium tetrachloride in tetrahydrofuran 2.5 h; Heating;
参考文献
Vellemaee, Eerold; Lebedev, Oleg; Maeeorg, Uno
Tetrahedron Letters, 2008 , vol. 49, # 8 p. 1373 - 1375
反应条件
1: Et3N / methanol 2: 42 percent / TfOH / CH2Cl2 / 1 h / 50 °C 3: KOH / dimethylsulfoxide / 140 °C View Scheme
参考文献
Tokuyama, Hidetoshi; Sato, Masashi; Ueda, Toshihiro; Fukuyama, Tohru
Heterocycles, 2001 , vol. 54, # 1 p. 105 - 108
反应条件
1: glacial acetic acid; nitric acid / 10 - 22 °C 2: bei der Verseifung View Scheme
参考文献
Reverdin
Chemische Berichte, 1909 , vol. 42, p. 1526
Chem. Zentralbl., 1909 , vol. 80, # I p. 1810
反应条件
1: water; acetic acid; nitric acid 2: diluted aq. NaOH solution 3: acetic acid; concentrated sulfuric acid View Scheme
参考文献
Uyeyanagi
Takeda Kenkyusho Nenpo, 1949 , vol. 8, p. 22,24,26
Chem.Abstr., 1953 , p. 4854
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=20°C; Cyclization; 3 h;
参考文献
Tohma, Hirofumi; Watanabe, Hiroaki; Takizawa, Shinobu; Maegawa, Tomohiro; Kita, Yasuyuki
Heterocycles, 1999 , vol. 51, # 8 p. 1785 - 1788
反应条件
1: potassium carbonate / dimethylformamide / 1 h / 20 °C 2: acetonitrile / 4 h / Irradiation View Scheme
参考文献
Halberkann
Chemische Berichte, 1921 , vol. 54, p. 1665 Anm.1
反应条件
1: [bis(acetoxy)iodo]benzene / 0.08 h / 25 °C / |Schlenk technique; |Inert atmosphere 2: bismuth trifluoromethanesulphonate / methanol / 25 °C / |Schlenk technique; |Inert atmosphere 3: zinc; trifluoroacetic acid / methanol / 25 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Zhang, Li; Wang, Weibin; Fan, Renhua
Organic Letters, 2013 , vol. 15, # 8 p. 2018 - 2021
反应条件
1: Et3N / methanol 2: 42 percent / TfOH / CH2Cl2 / 1 h / 50 °C View Scheme
参考文献
Tokuyama, Hidetoshi; Sato, Masashi; Ueda, Toshihiro; Fukuyama, Tohru
Heterocycles, 2001 , vol. 54, # 1 p. 105 - 108
反应条件
tert.-butylnitrite in acetonitrile T=45°C; 2.5 h; chemoselective reaction;
参考文献
Kilpatrick, Brenden; Heller, Markus; Arns, Steve
Chemical Communications, 2013 , vol. 49, # 5 p. 514 - 516
