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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
9-苯基咔唑
合成路线
（共 67 条）
609-73-4
2-硝基碘苯
→
反应条件
1150-62-5
9-苯基咔唑
反应条件
1.1: potassium phosphate; tetrakis(triphenylphosphine) palladium(0) / ethanol / 6 h / |Reflux; |Inert atmosphere 2.1: hydrazine hydrate / methanol / 2 h / 20 °C 3.1: hydrogenchloride; sodium nitrite / tetrahydrofuran; water / 0.33 h / |Cooling with ice 3.2: 20 °C / |Cooling with ice 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C 5.1: copper diacetate; sodium carbonate; ethylene glycol / isopropyl alcohol / 16 h / 85 °C / |Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 11-12 p. 2172 - 2178
86-00-0
2-硝基联苯
→
反应条件
1150-62-5
9-苯基咔唑
反应条件
1.1: hydrazine hydrate / methanol / 2 h / 20 °C 2.1: hydrogenchloride; sodium nitrite / tetrahydrofuran; water / 0.33 h / |Cooling with ice 2.2: 20 °C / |Cooling with ice 3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C 4.1: copper diacetate; sodium carbonate; ethylene glycol / isopropyl alcohol / 16 h / 85 °C / |Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 11-12 p. 2172 - 2178
90-41-5
邻氨基联苯
→
反应条件
1150-62-5
9-苯基咔唑
反应条件
1.1: hydrogenchloride; sodium nitrite / tetrahydrofuran; water / 0.33 h / |Cooling with ice 1.2: 20 °C / |Cooling with ice 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C 3.1: copper diacetate; sodium carbonate; ethylene glycol / isopropyl alcohol / 16 h / 85 °C / |Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 11-12 p. 2172 - 2178
591-50-4
碘苯
+
1413355-67-5
→
反应条件
1150-62-5
9-苯基咔唑
反应条件
in acetonitrile-D3 T=20°C; Ullmann Condensation; 10 h; Irradiation; Mechanism;
参考文献
Creutz, Sidney E.; Lotito, Kenneth J.; Fu, Gregory C.; Peters, Jonas C.
Science, 2012 , vol. 338, # 6107 p. 647 - 651
108-86-1
溴代苯
+
1413355-67-5
→
反应条件
1150-62-5
9-苯基咔唑
反应条件
in acetonitrile T=20°C; Ullmann Condensation; 10 h; Irradiation; Mechanism;
参考文献
Creutz, Sidney E.; Lotito, Kenneth J.; Fu, Gregory C.; Peters, Jonas C.
Science, 2012 , vol. 338, # 6107 p. 647 - 651
1413355-67-5
+
108-90-7
氯苯
→
反应条件
1150-62-5
9-苯基咔唑
反应条件
in acetonitrile T=20°C; Ullmann Condensation; 24 h; Irradiation; Mechanism;
参考文献
Creutz, Sidney E.; Lotito, Kenneth J.; Fu, Gregory C.; Peters, Jonas C.
Science, 2012 , vol. 338, # 6107 p. 647 - 651
75-09-2
二氯甲烷
+
603-34-9
→
反应条件
1150-62-5
9-苯基咔唑
+
10336-24-0
+
86-74-8
+
122-39-4
反应条件
aluminium trichloride T=70°C; 2 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 32, # 2 p. 275 - 280
603-34-9
+
71-43-2
→
反应条件
1150-62-5
9-苯基咔唑
+
86-74-8
+
122-39-4
反应条件
aluminium trichloride T=80°C; 24 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 32, # 2 p. 275 - 280
86844-02-2
→
反应条件
1150-62-5
9-苯基咔唑
反应条件
chloranil; xylene
参考文献
Journal of the Chemical Society, , p. 530,532
74497-02-2
→
反应条件
1150-62-5
9-苯基咔唑
反应条件
1: acetic acid / |Reflux 2: acetic acid / 19 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Asian Journal of Chemistry, , vol. 25, # 1 p. 501 - 504
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