1.1: N-ethyl-N,N-diisopropylamine / 4 h / 130 °C / |Inert atmosphere 2.1: sulfuric acid / methanol / 16 h / |Reflux 2.2: 2 h / pH 10 - 12 2.3: pH 4.5 View Scheme
参考文献
Ghislieri, Diego; Green, Anthony P.; Pontini, Marta; Willies, Simon C.; Rowles, Ian; Frank, Annika; Grogan, Gideon; Turner, Nicholas J.
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10863 - 10869
Multi-step reaction with 3 steps 1.1: dichloromethane / 2 h / 0 °C / |Inert atmosphere2.1: sodium hydroxide / 1 h / 100 °C / |Inert atmosphere2.2: 4 h / 100 °C / |Inert atmosphere3.1: N-ethyl-N,N-diisopropylamine; methanesulfonyl chloride / dichloromethane / 0 - 20 °C / |Inert atmosphere
参考文献
Ghislieri, Diego; Green, Anthony P.; Pontini, Marta; Willies, Simon C.; Rowles, Ian; Frank, Annika; Grogan, Gideon; Turner, Nicholas J. Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10863 - 10869
