2-(2-甲氧基苯甲酰基)苯甲酸合成路线 （共 12 条）
反应条件
n-butyllithium in tetrahydrofuran Cooling;
参考文献
Seo, Sangwon; Slater, Mark; Greaney, Michael F.
Organic Letters, 2012 , vol. 14, # 10 p. 2650 - 2653
反应条件
in tetrahydrofuran T=-100°C; 2 h;
参考文献
Parham; Bradsher; Edgar
Journal of Organic Chemistry, 1981 , vol. 46, # 6 p. 1057 - 1061
反应条件
diethyl ether; benzene
参考文献
Geyer
Journal of the American Chemical Society, 1942 , vol. 64, p. 2226
反应条件
hydrogenchloride Heatingovernight; Yield given;
参考文献
Edgar; Bradsher
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1585 - 1587
反应条件
1: 1.) BuLi / 1.) THF, -45 deg C, 2.) -100 deg C 2: 5percent aq. HCl / Heating; overnight View Scheme
参考文献
Edgar; Bradsher
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1585 - 1587
反应条件
1: 1.) BuLi / 1.) THF, -45 deg C, 2.) -100 deg C 2: 5percent aq. HCl / Heating; overnight View Scheme
参考文献
Edgar; Bradsher
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1585 - 1587
反应条件
sodium hydroxide; N-bromosuccinmide; meta-chloroperoxybenzoic acid 1.) CCl4, reflux, hν, 2 h; 2.) 20 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Harland, Philip A.; Hodge, Philip
Synthesis, 1983 , # 5 p. 419 - 421
反应条件
1: 48 h / 100 °C 2: 1.) NBS, benzoyl peroxide; 2.) aq. NaOH / 1.) CCl4, reflux, hν, 2 h; 2.) 20 deg C, 1 h View Scheme
参考文献
Harland, Philip A.; Hodge, Philip
Synthesis, 1983 , # 5 p. 419 - 421
反应条件
1: sulfuric acid / Diazotization.Eintragen der Diazoloesung in Schwefelsaeure bei 80grad 2: diluted KOH-solution View Scheme
参考文献
Sieglitz
Chemische Berichte, 1924 , vol. 57, p. 317
参考文献
Sieglitz
Chemische Berichte, 1924 , vol. 57, p. 317
