2-(4-甲氧基苯甲酰基)苯甲酸合成路线 (共 41 条)
反应条件
hydrogenchloride; aluminium trichloride in sodium carbonate; methoxybenzene; benzene
参考文献
Sterling Winthrop Inc.
Patent: US5380721 A1, 1995 ;
反应条件
n-butyllithium in tetrahydrofuran Cooling;
参考文献
Seo, Sangwon; Slater, Mark; Greaney, Michael F.
Organic Letters, 2012 , vol. 14, # 10 p. 2650 - 2653
反应条件
lithium hydroxide in tetrahydrofuran; water T=50°C; 2.5 h;
参考文献
Echavarren,A.M.; Stille,J.K.
Journal of the American Chemical Society, 1988 , vol. 110, p. 1557
反应条件
aluminium trichloride T=90°C; 4 h;
参考文献
Ghiaci; Bayat
Organic Preparations and Procedures International, 1996 , vol. 28, # 5 p. 609 - 612
反应条件
palladium (II) trifluoroacetate; silver carbonate in ethylene glycol dimethyl ether T=165°C; 48 h; Sealed tube; chemoselective reaction;
参考文献
Miao, Jinmin; Ge, Haibo
Organic Letters, 2013 , vol. 15, # 12 p. 2930 - 2933
反应条件
1: 64 percent / LiCl, 2,6-di-tert-butyl-4-methylphenol, 4 Angstroem molecular sieve / dichloro<1,1'-bis(diphenylphosphino)ferrocene>palladium(II) / dimethylformamide / 21 h / 90 °C / 2660 Torr 2: 100 percent / LiOH / tetrahydrofuran; H2O / 2.5 h / 50 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, p. 1557
反应条件
in tetrahydrofuran Grignard reaction;
参考文献
Mukaiyama, Teruaki; Yanagisawa, Manabu; Iida, Daisuke; Hachiya, Iwao
Chemistry Letters, 2000 , # 6 p. 606 - 607
反应条件
in tetrahydrofuran T=-100°C; 0.25 h;
参考文献
Parham; Bradsher; Edgar
Journal of Organic Chemistry, 1981 , vol. 46, # 6 p. 1057 - 1061
参考文献
Monatshefte fuer Chemie, , vol. 30, p. 486
反应条件
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: potassium carbonate / water; ethyl acetate / 4 h / 0 °C 3: palladium diacetate; boron trifluoride diethyl etherate; tert.-butylhydroperoxide; water / dimethyl sulfoxide; 1,4-dioxane / 130 °C 4: hydrogenchloride; water / dimethyl sulfoxide; 1,4-dioxane / 6 h / 100 °C View Scheme
参考文献
Chemical Communications, , vol. 49, # 82 p. 9464 - 9466