4-甲氧基-4-硝基二苯甲酮合成路线 (共 39 条)
反应条件
palladium 10 on activated carbon; triethylamine; triphenylphosphine in tetrahydrofuran T=80°C; 3 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 50, # 29 p. 4268 - 4271
反应条件
carbon; toluene-4-sulfonic acid T=90°C; Friedel-Crafts reaction; 4 h;
参考文献
Helvetica Chimica Acta, , vol. 88, # 8 p. 2282 - 2287
反应条件
3,3-dimethyl-butan-2-one; [Ru(CO)3Cl2]2; K3PO4*3H2O; [(t-Bu)3PH]BF4 in water; toluene T=100°C; 24 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 27 p. 7880 - 7882
反应条件
P2O5/silica gel in 1,2-dichloro-ethane Friedel Crafts acylation; 5 h; Reflux;
参考文献
Tetrahedron Letters, , vol. 49, # 47 p. 6715 - 6719
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2 in 1,4-dioxane T=100°C;
参考文献
Synlett, , # 2 p. 298 - 300
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 0.166667 h; Mechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 977 - 981
Zhurnal Organicheskoi Khimii, , vol. 18, # 6 p. 1131 - 1137
反应条件
1: 74 percent / NaOH / dimethylsulfoxide / 0.5 h / Ambient temperature 2: 86 percent / K2CO3, Bu4NBr / 1,2-dimethoxy-ethane / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 27, # 1 p. 135 - 144
反应条件
1: 74 percent / NaOH / dimethylsulfoxide / 0.5 h / Ambient temperature 2: 86 percent / K2CO3, Bu4NBr / 1,2-dimethoxy-ethane / Ambient temperature View Scheme
参考文献
Synthetic Communications, , vol. 27, # 1 p. 135 - 144
反应条件
phenyliodonium bis(phenylsulphonyl)methylide; copper acetylacetonate
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 379 - 382
反应条件
N(Et)4ClO4 in acetonitrile Electrolysis;
参考文献
Chemistry - A European Journal, , vol. 16, # 1 p. 178 - 188