3-溴-3-(4-硝基苯基)-3H-双吖丙啶合成路线 (共 7 条)
反应条件
sodium hypobromide; sodium bromide in water; dimethyl sulfoxide T=0°C; 3 h;
参考文献
Creary, Xavier; Sky, Anthony F.; Phillips, Gillian
Journal of Organic Chemistry, 1990 , vol. 55, # 7 p. 2005 - 2011
反应条件
1: 1) NaOMe, MeOH 2) NH4Cl / 1) r.t., 55 h 2) 43 deg C, 36 h 2: 11 percent / NaOBr, NaBr / dimethylsulfoxide; H2O / 3 h / 0 °C View Scheme
参考文献
Creary, Xavier; Sky, Anthony F.; Phillips, Gillian
Journal of Organic Chemistry, 1990 , vol. 55, # 7 p. 2005 - 2011
反应条件
in methanol T=25°C; Rate constant;
参考文献
Creary, Xavier; Sky, Anthony F.; Phillips, Gillian; Alonso, David E.
Journal of the American Chemical Society, 1993 , vol. 115, # 17 p. 7584 - 7592
反应条件
in dichloromethane T=0°C; 2 h; Irradiation;
参考文献
Barton, Derek H. R.; Jaszberenyi, Joseph Cs.; Theodorakis, Emmanouil A.; Reibenspies
Journal of the American Chemical Society, 1993 , vol. 115, # 18 p. 8050 - 8059
反应条件
in methanol
T=25°C; Rate constant;
参考文献
Creary, Xavier; Sky, Anthony F.; Phillips, Gillian; Alonso, David E.
Journal of the American Chemical Society, 1993 , vol. 115, # 17 p. 7584 - 7592
反应条件
in dichloromethane
T=0°C; 2 h; Irradiation;
参考文献
Barton, Derek H. R.; Jaszberenyi, Joseph Cs.; Theodorakis, Emmanouil A.; Reibenspies
Journal of the American Chemical Society, 1993 , vol. 115, # 18 p. 8050 - 8059
反应条件
in dichloromethane
T=0°C; 2 h; Irradiation;
参考文献
Barton, Derek H. R.; Jaszberenyi, Joseph Cs.; Theodorakis, Emmanouil A.; Reibenspies
Journal of the American Chemical Society, 1993 , vol. 115, # 18 p. 8050 - 8059