3-羟基-3-甲基戊二-d3酸酐合成路线 (共 3 条)
反应条件
acetic anhydride 18 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2989 - 2993
反应条件
1: 1) O3-O2; 2) 30percent aq. H2O2, H2SO4 / 1) ethyl acetate, -78 deg C; 2) H2O, 2 h, reflux 2: 76 percent / acetic anhydride / 18 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2989 - 2993
反应条件
sodium tetrahydroborate in isopropyl alcohol
24 h; Ambient temperature;
参考文献
Gill, Harjit K.; Smith, Roland W.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2989 - 2993