反应条件
<b>Multi-step reaction with 3 steps<br /> </b>1: NaCl, POCl<sub>3</sub> / 1.) 90 deg C, 20 min 2.)110 deg C, 2 h<br />2: 1,2,4-triazole, triethylamine, pyridine / acetonitrile / 2 h / Ambient temperature<br />3: Amberlyst 15 ion-exchange resin / H<sub>2</sub>O / 0.5 h / Ambient temperature<br /> <br />
参考文献
Davis, Andrew M.; Hall, Adrian D.; Williams, Andrew Journal of the American Chemical Society, 1988 , vol. 110, # 15 p. 5105 - 5108