Shields, Charles J.; Falvey, Daniel E.; Schuster, Gary B.; Buchardt, Ole; Nielsen, Peter E.
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3501 - 3507
1: thionyl chloride 2: 74 percent / aq. NaOH / 20 h / 0 °C 3: triethylamine / CH2Cl2 / 4 h / 0 °C 4: triethylamine / CH2Cl2 / 0 °C View Scheme
参考文献
Shields, Charles J.; Falvey, Daniel E.; Schuster, Gary B.; Buchardt, Ole; Nielsen, Peter E.
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3501 - 3507
1: 74 percent / aq. NaOH / 20 h / 0 °C 2: triethylamine / CH2Cl2 / 4 h / 0 °C 3: triethylamine / CH2Cl2 / 0 °C View Scheme
参考文献
Shields, Charles J.; Falvey, Daniel E.; Schuster, Gary B.; Buchardt, Ole; Nielsen, Peter E.
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3501 - 3507
1: triethylamine / CH2Cl2 / 4 h / 0 °C 2: triethylamine / CH2Cl2 / 0 °C View Scheme
参考文献
Shields, Charles J.; Falvey, Daniel E.; Schuster, Gary B.; Buchardt, Ole; Nielsen, Peter E.
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3501 - 3507
1: 1.) sodium nitrite, 2.) sodium azide / 1.) diazotization 2: thionyl chloride 3: 74 percent / aq. NaOH / 20 h / 0 °C 4: triethylamine / CH2Cl2 / 4 h / 0 °C 5: triethylamine / CH2Cl2 / 0 °C View Scheme
参考文献
Shields, Charles J.; Falvey, Daniel E.; Schuster, Gary B.; Buchardt, Ole; Nielsen, Peter E.
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3501 - 3507
