1-硫杂环癸-3,8-二炔合成路线 （共 4 条）
反应条件
sodium sulfide; caesium carbonate in ethanol; toluene Heating;
参考文献
Gleiter, Rolf; Rittinger, Stefan; Langer, Heinrich
Chemische Berichte, 1991 , vol. 124, # 2 p. 357 - 363
反应条件
1: 75 percent / CBr4, n-Bu3P / diethyl ether / 0.25 h / 0 °C 2: 9 percent / Na2S*Al2O3 / ethanol; CH2Cl2 / 18 h View Scheme
参考文献
Gleiter, Rolf; Rittinger, Stefan; Langer, Heinrich
Chemische Berichte, 1991 , vol. 124, # 2 p. 357 - 363
反应条件
1: pyridinium p-toluenesulfonate / methanol / 18 h 2: 75 percent / CBr4, n-Bu3P / diethyl ether / 0.25 h / 0 °C 3: 9 percent / Na2S*Al2O3 / ethanol; CH2Cl2 / 18 h View Scheme
参考文献
Nicolaou; Zuccarello; Riemer; Estevez; Dai
Journal of the American Chemical Society, 1992 , vol. 114, # 19 p. 7360 - 7371
反应条件
2: Na2S*9H2O, Cs2CO3 / ethanol; benzene View Scheme
参考文献
Gleiter, Rolf; Rittinger, Stefan
Tetrahedron Letters, 1988 , vol. 29, # 36 p. 4529 - 4532
