2-甲基-4-(N-甲基磺酰基)苯硼酸合成路线 （共 2 条）
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium acetate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane in 1,4-dioxane
T=100°C; Schlenk techniqueInert atmosphere;
参考文献
Almirall, S.A.; Vidal Juan, Bernat; Gonzalez Rodriguez, Jacob; Gual Roig, Silvia; Esteve Trias, Cristina; Vidal Gispert, Laura
Patent: EP2738172 A1, 2014 ;
Location in patent: Paragraph 0108; 0198 ;
反应条件
1: triethylamine / tetrahydrofuran; dichloromethane / 0 °C
2: potassium acetate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct / 1,4-dioxane / 100 °C / |Schlenk technique; |Inert atmosphere
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参考文献
Almirall, S.A.; Vidal Juan, Bernat; Gonzalez Rodriguez, Jacob; Gual Roig, Silvia; Esteve Trias, Cristina; Vidal Gispert, Laura
Patent: EP2738172 A1, 2014 ;
