(2R,3S,4S,5S)-5-羟基-2,3,4-三(苄氧基)-5-[(苄氧基)甲基]-环己酮合成路线 (共 18 条)
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene T=100°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 57, # 13 p. 3642 - 3650
反应条件
1: With acetic anhydride; dimethyl sulfoxide T=20°C; 2: With zinc(II) chloride in tetrahydrofuran; water Heating;
参考文献
Tetrahedron, , vol. 56, # 37 p. 7109 - 7122
反应条件
1: With acetic anhydride; dimethyl sulfoxide T=20°C; 24 h; 2: With zinc(II) chloride in tetrahydrofuran; water 4 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 37 p. 7109 - 7122
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-78 - 20°C; 7 h;
参考文献
Organic Letters, , vol. 8, # 18 p. 3935 - 3938
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene T=100°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 57, # 13 p. 3642 - 3650
反应条件
zinc(II) chloride in tetrahydrofuran; water 4 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 37 p. 7109 - 7122
反应条件
zinc(II) chloride in tetrahydrofuran; water 4 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 37 p. 7109 - 7122
反应条件
2-tert-butylimino-2-diethylamino-1,3-dimethylperhydro-1,3,2-diazaphosphorine in tetrahydrofuran T=0°C; 5 h;
参考文献
Organic Letters, , vol. 8, # 18 p. 3935 - 3938
反应条件
hydrogenchloride in tetrahydrofuran; water T=20°C; 0.5 h;
参考文献
Tetrahedron, , vol. 56, # 37 p. 7109 - 7122
反应条件
potassium hexamethylsilazane in tetrahydrofuran T=-78°C;
参考文献
Organic Letters, , vol. 8, # 18 p. 3935 - 3938