(氯二氟甲基)三甲基硅烷合成路线 （共 26 条）
反应条件
potassium hydroxide in water; toluene
T=50°C; 4 h; Inert atmosphereSealed tube;
参考文献
Wang, Fei; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 344 - 351
反应条件
potassium hydroxide in water; toluene
T=50°C; 4 h; Inert atmosphereSealed tube;
参考文献
Wang, Fei; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 344 - 351
反应条件
triphenylphosphine in tetrahydrofuran
T=70°C; Wittig Olefination; 10 h; Sealed tube;
参考文献
Wang, Fei; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 344 - 351
反应条件
potassium hydroxide in water; toluene
T=50°C; 4 h; Inert atmosphereSealed tube;
参考文献
Wang, Fei; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 344 - 351
反应条件
1-methyl-pyrrolidin-2-one; hydrogen fluoride; tetrabutyl ammonium fluoride
1.) THF, room temperature, 24 h, 2.) acetonitrile, water; Yield given. Multistep reaction;
参考文献
Yudin, Andrei K.; Prakash, G. K. Surya; Deffieux, Denis; Bradley, Michael; Bau, Robert; Olah, George A.
Journal of the American Chemical Society, 1997 , vol. 119, # 7 p. 1572 - 1581
反应条件
triphenylphosphine in tetrahydrofuran
T=70°C; Wittig Olefination; 10 h; Sealed tube;
参考文献
Wang, Fei; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 344 - 351
