in chloroform byproducts: H2O; suspn. of trans-OsO2(AsPh3)2Cl2 and CF3COOH in chloroform refluxed for 2h; excess solvent distilled off from react. mixt.; residue dissolved in CHCl3; complex pptd. with hexane; complex dried in vac. over KOH; elem. anal.;
参考文献
Belyaev; Eremin; Simanova; Evreinova
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, 2004 , vol. 30, # 4 p. 262 - 268
hydrogenchloride in dichloromethane Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 650 - 652
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 700 - 702
in chloroform byproducts: H2O; suspn. of trans-OsO2(AsPh3)2Cl2 and C(CH3)3COOH in chloroform refluxed and then filtered; solvent distilled off from filtrate; residue dissolvedin chloroform and complex salted out with hexane; complex dried in vac. over KOH; elem. anal.;
参考文献
Belyaev; Eremin; Simanova; Evreinova
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, 2004 , vol. 30, # 4 p. 262 - 268
