(3aR,7aS)-四氢-1H-吲哚-2,7(3H,4H)-二酮合成路线 (共 3 条)
反应条件
1: oxalyl chloride / toluene / 1.5 h 2: liq. NH3 3: triethylamine / pentane / 0.5 h / 23 °C 4: I2 / tetrahydrofuran / 0.17 h 5: 1.) AgOCOCF3, H2O, 2.) pyridinium chlorochromate / 1.) nitromethane, 2.) CH2Cl2 View Scheme
参考文献
Knapp, Spencer; Levorse, Anthony T.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4006 - 4014
反应条件
1: triethylamine / pentane / 0.5 h / 23 °C 2: I2 / tetrahydrofuran / 0.17 h 3: 1.) AgOCOCF3, H2O, 2.) pyridinium chlorochromate / 1.) nitromethane, 2.) CH2Cl2 View Scheme
参考文献
Knapp, Spencer; Levorse, Anthony T.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4006 - 4014
反应条件
1: liq. NH3 2: triethylamine / pentane / 0.5 h / 23 °C 3: I2 / tetrahydrofuran / 0.17 h 4: 1.) AgOCOCF3, H2O, 2.) pyridinium chlorochromate / 1.) nitromethane, 2.) CH2Cl2 View Scheme
参考文献
Knapp, Spencer; Levorse, Anthony T.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 4006 - 4014