反应条件
1: 1) PDC, 2) 5percent HCl / 1) CH2Cl2, RT, overnight, 2) MeOH, overnight 2: 52 percent / Zn(Hg), TMSCl / tetrahydrofuran / 12 h / Ambient temperature 3: 93 percent / OsO4, NMMNO / tetrahydrofuran; H2O; 2-methyl-propan-2-ol / 22 h / Ambient temperature View Scheme
参考文献
Zhou, Wei-shan; Jiang, Biao; Pan, Xin-fu
Tetrahedron, 1990 , vol. 46, # 9 p. 3173 - 3188
