2-甲基-2-丙基(2S)-3-丁烯-2-基氨基甲酸酯合成路线 (共 4 条)
反应条件
1: With ozone in methanol; dichloromethane T=-78°C; 0.166667 h; 2: With triphenylphosphine in methanol; dichloromethane Further stages.;
参考文献
Foerster, Sebastian; Helmchen, Guenter
Synlett, 2008 , # 6 p. 831 - 836
反应条件
Yield given. Multistep reaction;
参考文献
Moriwake, Toshio; Hamano, Shin-ich; Saito, Seiki; Torii, Shigeru; Kashino, Setsuo
Journal of Organic Chemistry, 1989 , vol. 54, # 17 p. 4114 - 4120
反应条件
1: 1.) 9-BBN, 2.) H2O2, NaOH / 1.) THF 2: 61 percent / PDC / dimethylformamide View Scheme
参考文献
Alcon, Montserrat; Canas, Marc; Poch, Marta; Moyano, Albert; Pericas, Miquel A.; Riera, Antoni
Tetrahedron Letters, 1994 , vol. 35, # 10 p. 1589 - 1592
反应条件
1: 1.) 9-BBN, 2.) H2O2, NaOH / 1.) THF
2: 61 percent / PDC / dimethylformamide
3: diethyl ether
View Scheme
参考文献
Alcon, Montserrat; Canas, Marc; Poch, Marta; Moyano, Albert; Pericas, Miquel A.; Riera, Antoni
Tetrahedron Letters, 1994 , vol. 35, # 10 p. 1589 - 1592