正庚基 2-乙酰氨基-3,4,6-O-三乙酰基-2-脱氧-beta-D-吡喃葡萄糖苷合成路线 (共 5 条)
反应条件
cobalt(II) chloride in dichloromethane T=42°C; 2.5 h; ConcentrationTimeTemperature;
参考文献
Kuryanov; Luschtshyk; Chupakhina
Russian Journal of Bioorganic Chemistry, 2013 , vol. 39, # 4 p. 426 - 433
Biokhimiya (Moscow), 2013 , vol. 39, # 4 p. 477 - 485
反应条件
toluene-4-sulfonic acid in 1,2-dichloro-ethane Heating;
参考文献
Zemyakov, A. E.; Chirva, V. Ya.
Chemistry of Natural Compounds, 1987 , vol. 23, # 5 p. 595 - 599
Khimiya Prirodnykh Soedinenii, 1987 , vol. 23, # 5 p. 714 - 718
反应条件
3 A molecular sieve; mercury(II) iodide in 1,2-dichloro-ethane Ambient temperature;
参考文献
Zemlyakov; Kur'yanov; Chirva
Chemistry of Natural Compounds, 1996 , vol. 32, # 3 p. 352 - 355
反应条件
cobalt(II) chloride in dichloromethane T=50°C; 36 h;
参考文献
Kuryanov; Luschtshyk; Chupakhina
Russian Journal of Bioorganic Chemistry, 2013 , vol. 39, # 4 p. 426 - 433
Biokhimiya (Moscow), 2013 , vol. 39, # 4 p. 477 - 485
反应条件
1: potassium carbonate / acetonitrile / 20 °C 2: cobalt(II) chloride / dichloromethane / 2.5 h / 42 °C View Scheme
参考文献
Russian Journal of Bioorganic Chemistry, , vol. 39, # 4 p. 426 - 433
Biokhimiya (Moscow), , vol. 39, # 4 p. 477 - 485