4-硝基苯酸(2S)-(+)-缩水甘油基合成路线 （共 9 条）
反应条件
pyridine; chloroform
参考文献
Journal of the American Chemical Society, , vol. 64, p. 1291
反应条件
sodium hydride in dichloromethane 0.5 h; Ambient temperature; Yield given;
参考文献
Synthesis, , # 3 p. 225 - 227
反应条件
1: 99 percent / glucose / ethanol; dimethylsulfoxide / 24 h / 30 °C / bakers' yeast, pH=6 2: pyridine / CH2Cl2 / 12 h / Ambient temperature 3: NaH / CH2Cl2 / 0.5 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 3 p. 225 - 227
反应条件
1: pyridine / CH2Cl2 / 12 h / Ambient temperature 2: NaH / CH2Cl2 / 0.5 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 3 p. 225 - 227
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 109, # 19 p. 5765 - 5780
反应条件
tetrabutyl ammonium fluoride 1) THF, 6 h, RT, 2) THF; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 558, # 1-2 p. 227 - 230
反应条件
15-crown-5; lipasePS-C 1.) CH3CN, 12 h, room temp., 2.) THF, water, 13 h, room temp.; Multistep reaction. Title compound not separated from byproducts;
参考文献
Synthetic Communications, , vol. 29, # 15 p. 2559 - 2566
反应条件
N,N-bis-2-(hydroxyethyl)-2-amino ethane sulfonic acid; esterase from Streptomyces diastatochromogenes in water T=25°C; pH=7.20; Enzyme kinetics;
参考文献
Liu, Andrew Man Fai; Somers, Neil A.; Kazlauskas, Romas J.; Brush, Terry S.; Zocher, Frank; Enzelberger, Markus M.; Bornscheuer, Uwe T.; Horsman, Geoff P.; Mezzetti, Alessandra; Schmidt-Dannert, Claudia; Schmid, Rolf D.
Tetrahedron Asymmetry, 2001 , vol. 12, # 4 p. 545 - 556
反应条件
N,N-bis-2-(hydroxyethyl)-2-amino ethane sulfonic acid; esterase from Streptomyces diastatochromogenes in water T=25°C; pH=7.20; Enzyme kinetics;
参考文献
Liu, Andrew Man Fai; Somers, Neil A.; Kazlauskas, Romas J.; Brush, Terry S.; Zocher, Frank; Enzelberger, Markus M.; Bornscheuer, Uwe T.; Horsman, Geoff P.; Mezzetti, Alessandra; Schmidt-Dannert, Claudia; Schmid, Rolf D.
Tetrahedron Asymmetry, 2001 , vol. 12, # 4 p. 545 - 556
