in neat (no solvent)
heated under flowing N2 atm. with flow rate of 30-100 cm**3/min to 750°C in Pt or alumina (to 450°C) pans at heating rate of 5-30°C/min;
参考文献
Nazli DIncer Kaya; Svoboda, Ingrid; Atakol, Orhan; Ergun, Uemit; Kenar, Adnan; Sari, Musa; Emreguel, Kaan C.
Journal of Thermal Analysis and Calorimetry, 2008 , vol. 92, # 2 p. 617 - 624
