双(2-硝基苯基)二硫化物合成路线 （共 240 条）
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; reductive cyclocondensation; 3 h;
参考文献
Chen; Zhong; Zhang
Journal of Chemical Research - Part S, 2000 , # 8 p. 386 - 387
反应条件
1: Na2S; NaOH; aqueous alcohol / Behandeln des Reaktionsprodukts mit Chloressigsaeureaethylester
2: hydrogen peroxide; glacial acetic acid
View Scheme
参考文献
Claasz
Chemische Berichte, 1912 , vol. 45, p. 1031
Chemische Berichte, 1916 , vol. 49, p. 1143
反应条件
1: zinc; acetic acid; aqueous HCl
View Scheme
参考文献
Bertoglio Riolo
Annali di Chimica (Rome, Italy), 1955 , vol. 45, p. 1174,1176
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; 6 h;
参考文献
Zhong; Zhang; Chen
Journal of the Indian Chemical Society, 2001 , vol. 78, # 6 p. 316 - 318
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; 4 h;
参考文献
Zhong; Zhang; Chen
Journal of the Indian Chemical Society, 2001 , vol. 78, # 6 p. 316 - 318
反应条件
1: With sodium tetrahydroborate in tetrahydrofuran
T=20°C; 2 h;
2: With water in tetrahydrofuran
T=0°C;
参考文献
Turos, Edward; Revell, Kevin D.
Patent: US2008/182815 A1, 2008 ;
Location in patent: Page/Page column 9 ;
反应条件
1: 2,2'-dinitrodiphenyl disulphide With samarium diiodide in tetrahydrofuran
T=20°C; 0.166667 h;
2: α-Bromo-benzeneacetic acid methyl ester in tetrahydrofuran
T=60°C; 4 h;
参考文献
Zhong, Weihui; Zhang, Yongmin
Tetrahedron Letters, 2001 , vol. 42, # 17 p. 3125 - 3127
反应条件
1: sodium tetrahydroborate / tetrahydrofuran / 50 °C / |Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C / |Inert atmosphere; |Cooling with ice
View Scheme
参考文献
Dornan, Peter K.; Kou, Kevin G. M.; Houk; Dong, Vy M.
Journal of the American Chemical Society, 2014 , vol. 136, # 1 p. 291 - 298
反应条件
1: 2,2'-dinitrodiphenyl disulphide With samarium; titanium tetrachloride in tetrahydrofuran
T=20°C; 0.5 h;
2: Benzalacetophenone in tetrahydrofuran
T=20°C; 4 h;
参考文献
Zhong, Weihui; Chen, Xiaoyuan; Zhang, Yongmin
Heteroatom Chemistry, 2001 , vol. 12, # 3 p. 156 - 160
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; 2 h;
参考文献
Zhong; Zhang; Chen
Journal of the Indian Chemical Society, 2001 , vol. 78, # 6 p. 316 - 318
