2-(苯甲酰氨基)-3-苯基败脂酸合成路线 (共 35 条)
反应条件
T=120°C; im geschlossenen Rohr;
参考文献
Ploechl
Chemische Berichte, 1883 , vol. 16, p. 2815
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Erlenmeyer; Lux
Chemische Berichte, 1898 , vol. 31, p. 2220
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Erlenmeyer; Kunlin
Justus Liebigs Annalen der Chemie, 1899 , vol. 307, p. 161
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Erlenmeyer; Knight
Chemische Berichte, 1894 , vol. 27, p. 2223
参考文献
Ploechl
Chemische Berichte, 1883 , vol. 16, p. 2815
参考文献
Erlenmeyer jun.
Justus Liebigs Annalen der Chemie, 1892 , vol. 271, p. 161
反应条件
T=130 - 140°C; 0.5 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 25, p. 762 - 764
反应条件
1) 130-140 deg C; 30 min; 2) 160-170 deg C; 30 min; Yield given. Multistep reaction;
参考文献
Ashare, Ram; Mukerjee, Arya K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 762 - 764
反应条件
isomer of mp: 200 degree;
参考文献
Carter; Risser
Journal of Biological Chemistry, 1941 , vol. 139, p. 255,260
反应条件
hydrogen; lt;(2R,3R)-2,3-Bis(diphenylphosphino)butangt;(π-norbornadien)rhodium(I)-perchlorate in tetrahydrofuran P=3000.2 Torr; 8 h; Yield given;
参考文献
Pullmann, Thomas; Engendahl, Barthel; Zhang, Ziyun; Hoelscher, Markus; Zanotti-Gerosa, Antonio; Dyke, Alan; Francio, Giancarlo; Leitner, Walter
Chemistry - A European Journal, 2010 , vol. 16, # 25 p. 7517 - 7526
反应条件
hydrogen; lt;Rh(NBD)2gt;ClO4; (2R,3S)-1,2-bis(diphenylphosphino)-3-tBoc-aminobutane in ethanol 22 h; Ambient temperature; Yield given;
参考文献
Yatagai; Zama; Yamagishi; Hida
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 739 - 746
反应条件
hydrogen; methyl 4-O-(diphenylphosphino)-2,3-O-isopropylidene-α-L-rhamnopyranoside; triethylamine; [{Rh(μ-Cl)(1,5-cyclooctadiene)}2] in ethanol; benzene 24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yamashita, Mitsuji; Kobayashi, Mineaki; Tsunekawa, Kenji; Sugiura, Motoyuki; Oshikawa, Tatsuo; et al.
Carbohydrate Research, 1984 , vol. 131, p. C6 - C7
反应条件
1: palladium/charcoal; ethanol / Hydrogenation 2: soil bacteria View Scheme
参考文献
Kameda et al.
Yakugaku Zasshi, 1958 , vol. 78, p. 767
Chem.Abstr., 1958 , p. 18237