反应条件
1: acetic acid; N-bromosuccinmide / 5 h / 10 - 20 °C
2: trifluoroacetic acid / dichloromethane / 2 h / 10 - 20 °C
3: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran; N,N-dimethyl-formamide / 10 h / 20 °C
View Scheme
参考文献
MYREXIS, INC.; BAJJI, Ashok, C.; TANGALLAPALLY, Rajendra, P.; KIM, In, Chul; KIM, Se, Ho; PARKER, Daniel, P.; TROVATO, Richard; PAPAC, Damon, I.; YAGER, Kraig; BAICHWAL, Vijay, R.
Patent: WO2012/148550 A1, 2012 ;
