in methanol Heatingequilibrium; var. solv.; Product distribution;

Multi-step reaction with 7 steps 1: 42 percent / imidazole / dimethylformamide / 1.5 h / 20 °C2: sodium hydrogen carbonate / aq. ethanol / 1.5 h / Heating3: N-methylmorpholine N-oxide monohydrate, selenium dioxide / CH2Cl2; methanol / 0.83 h / Heating4: imidazole / dimethylformamide / 1.5 h / 20 °C5: liq. SO2 / diethyl ether / 0.5 h / Heating6: 1.) ozone 2.) PPh3 / 1.) CH2Cl2, MeOH, -60 deg C, 40 min. 2.) CH2Cl2, MeOH, -60 to 0 deg C7: 5 percent / NaHCO3 / ethanol / 1.5 h / Heating  

Multi-step reaction with 3 steps 1: liq. SO2 / diethyl ether / 0.5 h / Heating2: 1.) ozone 2.) PPh3 / 1.) CH2Cl2, MeOH, -60 deg C, 40 min. 2.) CH2Cl2, MeOH, -60 to 0 deg C3: 5 percent / NaHCO3 / ethanol / 1.5 h / Heating  

Multi-step reaction with 5 steps 1: N-methylmorpholine N-oxide monohydrate, selenium dioxide / CH2Cl2; methanol / 0.83 h / Heating2: imidazole / dimethylformamide / 1.5 h / 20 °C3: liq. SO2 / diethyl ether / 0.5 h / Heating4: 1.) ozone 2.) PPh3 / 1.) CH2Cl2, MeOH, -60 deg C, 40 min. 2.) CH2Cl2, MeOH, -60 to 0 deg C5: 5 percent / NaHCO3 / ethanol / 1.5 h / Heating