反应条件
1: 95 percent / 1M sodium hydroxide / H2O / RT, 24 h, reflux, 3 h
2: 55 percent / cc sulphuric acid / 4.5 h / Heating
3: 83 percent / N-methylmorpholine, PCl5 / CCl4 / -10 deg C / 5 deg C, 1 h, 0, deg C / 5 deg C, 2 h
View Scheme
参考文献
Merrett, John H.; Spurden, William C.; Thomas, W Anthony; Tong, Brian P.; Whitcombe, Ian W. A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 61 - 68