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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
115764-98-2
合成路线
（共 6 条）
115103-03-2
+
1068-57-1
乙酰肼
→
反应条件
115764-98-2
反应条件
in butan-1-ol 7.5 h; Heating;
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
93-17-4
(3,4-二甲氧苯基)乙腈
→
反应条件
115764-98-2
反应条件
1: 75 percent / KOH / benzene; methanol; H2O / 3 h / Ambient temperature 2: Fe / ethanol; H2O; acetic acid / 2 h / Heating 3: 99 percent / CHCl3 4: 1. N2H4; 2. aq. NH3 / 1. pyridine, ethanol, H2O, 60 to 65 deg C, 2 h; 2. H2O, 20 min 5: 78 percent / P2S5 / pyridine / 0.75 h / Heating 6: 64 percent / butan-1-ol / 7.5 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
94100-07-9
→
反应条件
115764-98-2
反应条件
1: 99 percent / CHCl3 2: 1. N2H4; 2. aq. NH3 / 1. pyridine, ethanol, H2O, 60 to 65 deg C, 2 h; 2. H2O, 20 min 3: 78 percent / P2S5 / pyridine / 0.75 h / Heating 4: 64 percent / butan-1-ol / 7.5 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
94100-08-0
→
反应条件
115764-98-2
反应条件
1: Fe / ethanol; H2O; acetic acid / 2 h / Heating 2: 99 percent / CHCl3 3: 1. N2H4; 2. aq. NH3 / 1. pyridine, ethanol, H2O, 60 to 65 deg C, 2 h; 2. H2O, 20 min 4: 78 percent / P2S5 / pyridine / 0.75 h / Heating 5: 64 percent / butan-1-ol / 7.5 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
105278-81-7
→
反应条件
115764-98-2
反应条件
1: 78 percent / P2S5 / pyridine / 0.75 h / Heating 2: 64 percent / butan-1-ol / 7.5 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
100-00-5
对硝基氯苯
→
反应条件
115764-98-2
反应条件
1: 75 percent / KOH / benzene; methanol; H2O / 3 h / Ambient temperature 2: Fe / ethanol; H2O; acetic acid / 2 h / Heating 3: 99 percent / CHCl3 4: 1. N2H4; 2. aq. NH3 / 1. pyridine, ethanol, H2O, 60 to 65 deg C, 2 h; 2. H2O, 20 min 5: 78 percent / P2S5 / pyridine / 0.75 h / Heating 6: 64 percent / butan-1-ol / 7.5 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
