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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
115764-99-3
合成路线
（共 5 条）
74085-88-4
+
115103-04-3
→
反应条件
115764-99-3
反应条件
in pyridine; butan-1-ol 6 h; Heating;
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
94100-09-1
→
反应条件
115764-99-3
反应条件
1: 65.2 g / CHCl3 / 7 h / Heating 2: 1. N2H4; 2. aq. NH3 / 1. methanol, H2O, 60 to 65 deg C, 3 h; 2. water, room temperature, 1 h 3: 75 percent / P2S5 / pyridine / 0.75 h / Heating 4: 89 percent / pyridine; butan-1-ol / 6 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
94100-10-4
→
反应条件
115764-99-3
反应条件
1: 98 percent / Fe / ethanol; H2O; acetic acid / 2 h / Heating 2: 65.2 g / CHCl3 / 7 h / Heating 3: 1. N2H4; 2. aq. NH3 / 1. methanol, H2O, 60 to 65 deg C, 3 h; 2. water, room temperature, 1 h 4: 75 percent / P2S5 / pyridine / 0.75 h / Heating 5: 89 percent / pyridine; butan-1-ol / 6 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
105278-83-9
→
反应条件
115764-99-3
反应条件
1: 75 percent / P2S5 / pyridine / 0.75 h / Heating 2: 89 percent / pyridine; butan-1-ol / 6 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
105278-84-0
→
反应条件
115764-99-3
反应条件
1: 1. N2H4; 2. aq. NH3 / 1. methanol, H2O, 60 to 65 deg C, 3 h; 2. water, room temperature, 1 h 2: 75 percent / P2S5 / pyridine / 0.75 h / Heating 3: 89 percent / pyridine; butan-1-ol / 6 h / Heating View Scheme
参考文献
Vejdelek, Zdenek; Holubek, Jiri; Budesinsky, Milos; Ryska, Miroslav; Svatek, Emil; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 361 - 372
