5-(氯乙酰基)-2-羟基苯甲醛合成路线 （共 3 条）
反应条件
AlCl3, aluminium chloride in dichloromethane T=0°C; 48 h; Reflux;
参考文献
Shenyang J and Health Pharmaceutical Co., Ltd.
Patent: EP2468730 A1, 2012 ;
Location in patent: Page/Page column 18 ;
反应条件
aluminium trichloride in dichloromethane 16 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Babad; Carruthers; Jaret; Steinman
Synthesis, 1988 , # 12 p. 966 - 972
反应条件
1: 75 percent / propan-2-ol / 18 h / Ambient temperature 2: 2.) 12M aq. HCl / 1.) 2-propanol, reflux, 2 h, 2.) 18 h 3: NaOCH3 / methanol / 0.08 h / 0 °C 4: H2 / 5percent Pd/c / methanol / 10 h / 3102.9 Torr View Scheme
参考文献
Babad; Carruthers; Jaret; Steinman
Synthesis, 1988 , # 12 p. 966 - 972
