3-[(叔丁基亚磺酰基)亚氨基]氧杂环丁烷合成路线 (共 2 条)
反应条件
titanium(IV) isopropylate in dichloromethane T=20°C; Inert atmosphereReflux;
参考文献
Jung, Hyung Hoon; Buesking, Andrew W.; Ellman, Jonathan A.
Organic Letters, 2011 , vol. 13, # 15 p. 3912 - 3915
反应条件
1: 3,3-dimethoxyoxetane in dichloromethane T=48°C; 72 h; Inert atmosphere; 2: (S)-(-)-2-methyl-2-propanesulfinamide With titanium tetraethoxide in tetrahydrofuran T=50°C; 5 h; Inert atmosphere;
参考文献
Hamzik, Philip J.; Brubaker, Jason D.
Organic Letters, 2010 , vol. 12, # 5 p. 1116 - 1119