2-噻吩硼酸甲基亚氨基二乙酸酯合成路线 (共 4 条)
反应条件
in dimethyl sulfoxide; benzene 8 h; Reflux;
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS; BURKE, Martin, D.; KNAPP, David, M.; GILLIS, Eric, P.
Patent: WO2010/36921 A2, 2010 ;
Location in patent: Page/Page column 35 ;
反应条件
sodium hydroxide in tetrahydrofuran; water T=23°C; 0.333333 h;
参考文献
Knapp, David M.; Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2009 , vol. 131, p. 6961 - 6963
反应条件
in not given hydrolysis of appropriate N-methyliminodiacetic acid boronate;
参考文献
Knapp, David M.; Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2009 , vol. 131, p. 6961 - 6963
反应条件
1: With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate in 1,4-dioxane
T=23°C; 0.166667 h; Inert atmosphere;
2: With potassium phosphate; water in 1,4-dioxane
T=23 - 60°C; 6.5 h; Inert atmosphere;
参考文献
Knapp, David M.; Gillis, Eric P.; Burke, Martin D.
Journal of the American Chemical Society, 2009 , vol. 131, p. 6961 - 6963