Jacobi, Bridey Grant; Laitar, David S.; Pu, Lihung; Wargocki, Michael F.; DiPasquale, Antonio G.; Fortner, Kevin C.; Schuck, Stephany M.; Brown, Seth N.
Inorganic Chemistry, 2002 , vol. 41, # 18 p. 4815 - 4823
in 1,2-dichloro-ethane
the ligand compd. was dissolved in hot 1,2-dichloroethane and powd. HgCl2 was added (molar ratio Hg:P = 1:2); after a few minutes the soln. cleared and it was allowed to cool; the crude product was filtered off and washed with Et2O; elem. anal.;
参考文献
Allman, Tim; Goel, Ram G.
Canadian Journal of Chemistry, 1984 , vol. 62, p. 615 - 620
in tetrahydrofuran; dichloromethane
a soln. of HgCl2 in THF was added to a soln. of the ligand in CH2Cl2; the soln. was reduced in vol. and a small amt. of Et2O was added; recrystn. from CH2Cl2/Et2O; elem. anal.;
参考文献
Allman, Tim; Goel, Ram G.
Canadian Journal of Chemistry, 1984 , vol. 62, p. 615 - 620
1: hydrogen tetrachloroaurate(III) tetrahydrate With di-n-propyl sulfide in ethanol
T=40°C; 0.166667 h;
2: tris(p-chloro phenyl)phosphine in ethanol
T=40°C; 1 h;
参考文献
Zalesskiy, Sergey S.; Sedykh, Alexander E.; Kashin, Alexey S.; Ananikov, Valentine P.
Journal of the American Chemical Society, 2013 , vol. 135, # 9 p. 3550 - 3559
Fukuzumi, Shunichi; Shimoosako, Kanji; Suenobu, Tomoyoshi; Watanabe, Yoshihito
Journal of the American Chemical Society, 2003 , vol. 125, # 30 p. 9074 - 9082
