(S)-()-N-烯丙基-α-甲基苄胺合成路线 （共 14 条）
反应条件
2-mercapto benzoic acid; 1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=60°C; 0.25 h;
参考文献
Lemaire-Audoire; Lemaire-Audoire, Sandrine; Savignac; Savignac, Monique; Genet; Genet, Jean Pierre; Bernard; Bernard, Jean-Marie
Tetrahedron Letters, 1995 , vol. 36, # 8 p. 1267 - 1270
反应条件
1: 89 percent / NaHCO3, sodium iodide / tetrahydrofuran; dimethylsulfoxide / Heating 2: 85 percent / 2-mercaptobenzoic acid, Pd(dba)2, DPPB / tetrahydrofuran / 20 °C View Scheme
参考文献
Lemarie-Audoire, Sandrine; Savignac, Monique; Dupuis, Christophe; Genet, Jean Pierre
Bulletin de la Societe Chimique de France, 1995 , vol. 132, p. 1157 - 1166
反应条件
2-mercapto benzoic acid; 1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran
T=20°C; 0.5 h;
参考文献
Lemaire-Audoire; Lemaire-Audoire, Sandrine; Savignac; Savignac, Monique; Genet; Genet, Jean Pierre; Bernard; Bernard, Jean-Marie
Tetrahedron Letters, 1995 , vol. 36, # 8 p. 1267 - 1270
反应条件
sodium carbonate in acetonitrile
T=20°C; 4 h;
参考文献
Rodriguez, Veronica; Sanchez, Mario; Quintero, Leticia; Sartillo-Piscil, Fernando
Tetrahedron, 2004 , vol. 60, # 48 p. 10809 - 10815
参考文献
Galeazzi, Roberta; Geremia, Silvano; Mobbili, Giovanna; Orena, Mario
Tetrahedron Asymmetry, 1996 , vol. 7, # 12 p. 3573 - 3584
反应条件
lithium in tetrahydrofuran; ammonia; tert-butyl alcohol
T=-60°C; Birch reduction; 0.5 h;
参考文献
Sugiyama, Shigeo; Morishita, Kenji; Ishii, Keitaro
Heterocycles, 2001 , vol. 55, # 2 p. 353 - 364
反应条件
lithium in tetrahydrofuran; ammonia; tert-butyl alcohol
T=-60°C; Birch reduction; 0.5 h;
参考文献
Sugiyama, Shigeo; Morishita, Kenji; Ishii, Keitaro
Heterocycles, 2001 , vol. 55, # 2 p. 353 - 364
反应条件
N,N'-dimethyl-(R)-1,1'-binaphthyldiamine-bis-2-pyridinecarboxyamide; trichlorosilane in dichloromethane
T=0°C; 12 h; Inert atmosphere; optical yield given as percent eestereoselective reaction;
参考文献
Guizzett, Stefania; Benaglia, Maurizio; Celentano, Giuseppe
European Journal of Organic Chemistry, 2009 , # 22 p. 3683 - 3687
反应条件
hantzsch ester; rac-VAPOL hydrogen phosphate in dichloromethane
T=15°C; 9 h; enantioselective reaction;
参考文献
Khan, Imran A.; Saxena, Anil K.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 11656 - 11669
反应条件
in tetrahydrofuran
24 h; Ambient temperature;
参考文献
Nakanishi, Saburo; Okamoto, Kenji; Yamaguchi, Hiroshi; Takata, Toshikazu
Synthesis, 1998 , # 12 p. 1735 - 1741
