(S)-()-N-烯丙基-α-甲基苄胺合成路线 （共 14 条）
反应条件
1: 77 percent / copper(I) chloride / dimethylformamide / 2.5 h / 20 °C
2: 28 percent / methylmagnesium bromide / tetrahydrofuran; diethyl ether / 5 h / -78 °C
3: 11 percent / lithium / liquid ammonia; 2-methyl-propan-2-ol; tetrahydrofuran / 0.5 h / -60 °C
View Scheme
参考文献
Sugiyama, Shigeo; Morishita, Kenji; Ishii, Keitaro
Heterocycles, 2001 , vol. 55, # 2 p. 353 - 364
反应条件
1: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C
2: rac-VAPOL hydrogen phosphate; hantzsch ester / dichloromethane / 9 h / 15 °C
View Scheme
参考文献
Khan, Imran A.; Saxena, Anil K.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 11656 - 11669
参考文献
Basha; McClellan; DeBernardis
Tetrahedron Letters, 1991 , vol. 32, # 40 p. 5469 - 5472
反应条件
in N,N-dimethyl-formamide
参考文献
Fernandez, Isabelle; Munoz, Luis
Tetrahedron Asymmetry, 2006 , vol. 17, # 17 p. 2548 - 2557
