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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
115982-19-9
合成路线
（共 9 条）
919082-35-2
→
反应条件
115982-19-9
反应条件
1: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 2: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
47811-27-8
→
反应条件
115982-19-9
反应条件
1: 62 percent / sodium hydrogen carbonate / acetonitrile / 18 h / Heating 2: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 3: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
19283-70-6
3,4-二甲氧基-2-羟基苯甲醛
→
反应条件
115982-19-9
反应条件
1: K2CO3 / acetone / 6 h / Heating 2: 84 percent / AcOH; ethylenediamine / 20 °C 3: 95 percent / LAH / tetrahydrofuran / 24 h / 20 °C 4: Na2CO3 / CH2Cl2; H2O / 2 h / 20 °C 5: 66 percent / POCl3 / dimethylformamide / 3 h / 20 °C 6: 62 percent / sodium hydrogen carbonate / acetonitrile / 18 h / Heating 7: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 8: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
5487-33-2
(3-苄氧基-4-甲氧基-苯基)乙酸
→
反应条件
115982-19-9
反应条件
1: (COCl)2; DMF / CH2Cl2 / 2 h / 20 °C 2: Na2CO3 / CH2Cl2; H2O / 2 h / 20 °C 3: 66 percent / POCl3 / dimethylformamide / 3 h / 20 °C 4: 62 percent / sodium hydrogen carbonate / acetonitrile / 18 h / Heating 5: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 6: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
54313-33-6
2-(3-(苄氧基)-4-甲氧基苯基)乙酰氯
→
反应条件
115982-19-9
反应条件
1: Na2CO3 / CH2Cl2; H2O / 2 h / 20 °C 2: 66 percent / POCl3 / dimethylformamide / 3 h / 20 °C 3: 62 percent / sodium hydrogen carbonate / acetonitrile / 18 h / Heating 4: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 5: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
35115-16-3
→
反应条件
115982-19-9
反应条件
1: 66 percent / POCl3 / dimethylformamide / 3 h / 20 °C 2: 62 percent / sodium hydrogen carbonate / acetonitrile / 18 h / Heating 3: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 4: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
121-33-5
香草醛
→
反应条件
115982-19-9
反应条件
1: 62 percent / sodium hydrogen carbonate / acetonitrile / 18 h / Heating 2: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 3: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
1034028-91-5
→
反应条件
115982-19-9
反应条件
1: 62 percent / sodium hydrogen carbonate / acetonitrile / 18 h / Heating 2: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 3: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
2103-57-3
2,3,4-三甲氧基苯甲醛
→
反应条件
115982-19-9
反应条件
1: 87 percent / AlCl3 / benzene 2: K2CO3 / acetone / 6 h / Heating 3: 84 percent / AcOH; ethylenediamine / 20 °C 4: 95 percent / LAH / tetrahydrofuran / 24 h / 20 °C 5: Na2CO3 / CH2Cl2; H2O / 2 h / 20 °C 6: 66 percent / POCl3 / dimethylformamide / 3 h / 20 °C 7: 62 percent / sodium hydrogen carbonate / acetonitrile / 18 h / Heating 8: hydrogen / Pd/C / ethyl acetate / 20 °C / 3878.61 Torr 9: NaH / tetrahydrofuran / 0 - 20 °C View Scheme
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
