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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
四氟乙烯
合成路线
（共 998 条）
116-14-3
四氟乙烯
+
100-58-3
溴化苯基镁
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
反应条件
tris-(dibenzylideneacetone)dipalladium(0); zinc(II) chloride; lithium iodide in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) T=40°C; P=2660.18 Torr; 8 h; Inert atmosphereAutoclave;
参考文献
Ohashi, Masato; Kambara, Tadashi; Hatanaka, Tsubasa; Saijo, Hiroki; Doi, Ryohei; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 10 p. 3256 - 3259
116-14-3
四氟乙烯
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
反应条件
caesium carbonate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) T=100°C; P=2660.18 Torr; 5 h;
参考文献
Ohashi, Masato; Saijo, Hiroki; Shibata, Mitsutoshi; Ogoshi, Sensuke
European Journal of Organic Chemistry, 2013 , # 3 p. 443 - 447
116-14-3
四氟乙烯
+
98-80-6
苯硼酸
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; tri-cyclo-hexyl-phosphine in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) T=100°C; 2 h; Inert atmosphere; Reagent/catalystTimeSolvent;
参考文献
Daikin Industries; Osaka University; Nagai, Takabumi; Adachi, Kenji; Shibanuma, Takashi; Ogoshi, Sensuke; Ohashi, Masato
Patent: US2013/324757 A1, 2013 ;
Location in patent: Paragraph 0309 ;
116-14-3
四氟乙烯
+
100-58-3
溴化苯基镁
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
+
569-72-2
1-(2,2-二氟-1-苯基乙烯基)-4-氟苯
反应条件
lithium iodide; tris-(dibenzylideneacetone)dipalladium(0); triphenylphosphine in tetrahydrofuran; diethyl ether; benzene-d6 T=60°C; P=2625.26 Torr; 2 h; Product distribution / selectivity;
参考文献
Nagai, Takabumi; Shibanuma, Takashi; Ogoshi, Sensuke; Ohashi, Masato
Patent: US2012/330072 A1, 2012 ;
Location in patent: Page/Page column 7 ;
116-14-3
四氟乙烯
+
5123-13-7
5,5-二甲基-2-苯基-1,3,2-二氧硼杂
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
+
569-72-2
1-(2,2-二氟-1-苯基乙烯基)-4-氟苯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate; tri-cyclo-hexyl-phosphine in tetrahydrofuran; benzene-d6 T=100°C; 16 h; Inert atmosphere;
参考文献
Daikin Industries; Osaka University; Nagai, Takabumi; Adachi, Kenji; Shibanuma, Takashi; Ogoshi, Sensuke; Ohashi, Masato
Patent: US2013/324757 A1, 2013 ;
Location in patent: Paragraph 0287 ;
116-14-3
四氟乙烯
+
5123-13-7
5,5-二甲基-2-苯基-1,3,2-二氧硼杂
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
+
20488-54-4
(E)-A,A’-二氟芪
+
569-72-2
1-(2,2-二氟-1-苯基乙烯基)-4-氟苯
+
20488-55-5
反应条件
bis(1,5-cyclooctadiene)nickel (0); caesium carbonate; tri-cyclo-hexyl-phosphine in tetrahydrofuran; benzene-d6 T=100°C; 16 h; Inert atmosphere;
参考文献
Daikin Industries; Osaka University; Nagai, Takabumi; Adachi, Kenji; Shibanuma, Takashi; Ogoshi, Sensuke; Ohashi, Masato
Patent: US2013/324757 A1, 2013 ;
Location in patent: Paragraph 0277-0284 ;
116-14-3
四氟乙烯
+
4406-77-3
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
反应条件
caesium carbonate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) T=100°C; P=2660.18 Torr; 5 h;
参考文献
Ohashi, Masato; Saijo, Hiroki; Shibata, Mitsutoshi; Ogoshi, Sensuke
European Journal of Organic Chemistry, 2013 , # 3 p. 443 - 447
116-14-3
四氟乙烯
+
182281-03-4
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
反应条件
caesium carbonate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) T=100°C; P=2660.18 Torr; 5 h;
参考文献
Ohashi, Masato; Saijo, Hiroki; Shibata, Mitsutoshi; Ogoshi, Sensuke
European Journal of Organic Chemistry, 2013 , # 3 p. 443 - 447
116-14-3
四氟乙烯
+
5123-13-7
5,5-二甲基-2-苯基-1,3,2-二氧硼杂
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
反应条件
bis(dibenzylideneacetone)-palladium(0); tri-iso-propyl phosphine in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) T=100°C; P=2660.18 Torr; 5 h; Catalytic behavior; SolventReagent/catalystConcentrationTemperatureTime;
参考文献
Ohashi, Masato; Saijo, Hiroki; Shibata, Mitsutoshi; Ogoshi, Sensuke
European Journal of Organic Chemistry, 2013 , # 3 p. 443 - 447
116-14-3
四氟乙烯
+
100-58-3
溴化苯基镁
→
反应条件
447-14-3
1,2,2-三氟苯乙烯
+
20488-54-4
(E)-A,A’-二氟芪
+
569-72-2
1-(2,2-二氟-1-苯基乙烯基)-4-氟苯
+
20488-55-5
反应条件
[Ni0(1,5-cyclooctadiene)2]; triphenylphosphine in tetrahydrofuran; diethyl ether T=20°C; P=2625.26 Torr; 48 h; Product distribution / selectivity;
参考文献
Nagai, Takabumi; Shibanuma, Takashi; Ogoshi, Sensuke; Ohashi, Masato
Patent: US2012/330072 A1, 2012 ;
Location in patent: Page/Page column 7 ;
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