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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
四氟乙烯
合成路线
（共 998 条）
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
865-86-1
1H,1H,2H,2H-全氟-1-十二醇
+
21652-58-4
1H,1H,2H-全氟-1-癸烯
+
678-39-7
1H,1H,2H,2H-全氟-1-癸醇
+
30389-25-4
1H,1H,2H-全氟-1-十二烯
+
27905-45-9
1H,1H,2H,2H-全氟癸基丙烯酸酯
+
17741-60-5
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9 ;
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
34395-24-9
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
34395-24-9
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9-10 ;
116-14-3
四氟乙烯
+
640723-20-2
→
反应条件
335-05-7
反应条件
in diethylene glycol soln. of educts, in presence of CsF, 80°C, 4 d;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
116-14-3
四氟乙烯
+
59529-67-8
→
反应条件
2154-59-8
+
79-38-9
反应条件
byproducts: SiF4; heated at 180°C, 17 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 4.2, page 41 - 49
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
865-86-1
1H,1H,2H,2H-全氟-1-十二醇
+
21652-58-4
1H,1H,2H-全氟-1-癸烯
+
678-39-7
1H,1H,2H,2H-全氟-1-癸醇
+
30389-25-4
1H,1H,2H-全氟-1-十二烯
+
27905-45-9
1H,1H,2H,2H-全氟癸基丙烯酸酯
+
17741-60-5
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9 ;
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
34395-24-9
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 8-9 ;
116-14-3
四氟乙烯
+
54509-73-8
+
354-64-3
五氟碘乙烷
+
10192-85-5
丙烯酸钾
→
反应条件
34395-24-9
反应条件
1: 1,1,2,2-tetrafluoroethylene; 1-iodo-pentafluoro-ethane With copper catalyst T=80°C; P=6000.6 Torr; 2: ethene With copper catalyst T=100°C; P=2250.23 Torr; 3 h; 3: acrylic acid potassium salt With 4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
Patent: EP1757574 A1, 2007 ;
Location in patent: Page/Page column 9-10 ;
116-14-3
四氟乙烯
→
反应条件
76-16-4
反应条件
NiF2; fluorine T=100°C;
参考文献
Zakharov, V. Yu.; Denisov, A. K.; Novikova, M. D.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 12 p. 1942 - 1945
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 12 p. 1844 - 1846
116-14-3
四氟乙烯
+
75-10-5
→
反应条件
354-33-6
+
76-16-4
+
677-56-5
反应条件
SbF5 T=-16 - -4°C; P=1644.4 - 5414.51 Torr; 1 h; Product distribution / selectivity;
参考文献
WO2008/8252 A1, ;
Page/Page column 8-9 ;
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