1-氨基-2-溴-4-羟基蒽醌合成路线 （共 15 条）
反应条件
bromine; boric acid in water
参考文献
Bayer Aktiengesellschaft
Patent: US4741867 A1, 1988 ;
反应条件
nitrogen; paraformaldehyde in water
反应条件
bromine T=50 - 60°C; Bio-ionic liquid;
参考文献
Phadtare, Sunanda Balaso; Shankarling, Ganapati Subray
Green Chemistry, 2010 , vol. 12, # 3 p. 458 - 462
反应条件
sulfuric acid; boric acid T=80 - 100°C; 1.5 h;
参考文献
Es'kin, A. P.; Gornostaev, L. M.; Zeibert, G. F.; Bogdanchikov, G. A.; El'tsov, A. V.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 162 - 167
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 188 - 194
反应条件
sulfuric acid T=100 - 110°C; 0.25 h;
参考文献
Sakilidi, V. T.; Gornostaev, L. M.
Journal of Organic Chemistry USSR (English Translation), 1982 , p. 939 - 942
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1084 - 1089
反应条件
sulfuric acid T=60 - 70°C; 0.5 h;
参考文献
Sakilidi, V. T.; Gornostaev, L. M.
Journal of Organic Chemistry USSR (English Translation), 1982 , p. 939 - 942
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1084 - 1089
反应条件
1: 71 percent / dioxane / 0.5 h / 20 - 25 °C 2: 80 percent / H2 / 0.2percent Pd/C / ethanol / 24 h / 40 - 50 °C / 760 Torr 3: 85 percent / 80percent H2SO4, H3BO3 / 1.5 h / 80 - 100 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 26, # 1.2 p. 162 - 167
Zhurnal Organicheskoi Khimii, , vol. 26, # 1 p. 188 - 194
反应条件
1: 80 percent / H2 / 0.2percent Pd/C / ethanol / 24 h / 40 - 50 °C / 760 Torr 2: 85 percent / 80percent H2SO4, H3BO3 / 1.5 h / 80 - 100 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 26, # 1.2 p. 162 - 167
Zhurnal Organicheskoi Khimii, , vol. 26, # 1 p. 188 - 194
反应条件
sulfuric acid T=100 - 110°C;
反应条件
1: 88 percent / acetic acid / 0.67 h / Heating 2: 74 percent / 90percent H2SO4 / 0.25 h / 100 - 110 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 939 - 942
Zhurnal Organicheskoi Khimii, , vol. 18, # 5 p. 1084 - 1089
