4,6,7-三甲氧基-8-甲基-2-萘羧酸甲酯合成路线 （共 6 条）
反应条件
potassium carbonate in acetone 24 h;
参考文献
Le, Tin Thanh; Chau, Nguyet Trang Thanh; Nguyen, Tai Tan; Brien, Josselin; Thai, Trieu Tien; Nourry, Arnaud; Castanet, Anne-Sophie; Nguyen, Kim Phi Phung; Mortier, Jacques
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 601 - 608
反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran 2.1: potassium tert-butylate / N,N-dimethyl-formamide / 20 °C 3.1: acetic anhydride; sodium carbonate / acetic acid / Reflux 3.2: Reflux 4.1: potassium carbonate / acetone / 24 h / 20 °C View Scheme
参考文献
Le, Tin Thanh; Chau, Nguyet Trang Thanh; Nguyen, Tai Tan; Brien, Josselin; Thai, Trieu Tien; Nourry, Arnaud; Castanet, Anne-Sophie; Nguyen, Kim Phi Phung; Mortier, Jacques
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 601 - 608
反应条件
1.1: potassium tert-butylate / N,N-dimethyl-formamide / 20 °C 2.1: acetic anhydride; sodium carbonate / acetic acid / Reflux 2.2: Reflux 3.1: potassium carbonate / acetone / 24 h / 20 °C View Scheme
参考文献
Le, Tin Thanh; Chau, Nguyet Trang Thanh; Nguyen, Tai Tan; Brien, Josselin; Thai, Trieu Tien; Nourry, Arnaud; Castanet, Anne-Sophie; Nguyen, Kim Phi Phung; Mortier, Jacques
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 601 - 608
反应条件
1.1: 2,2,6,6-tetramethylpiperidinyl-lithium 2.1: lithium aluminium tetrahydride / tetrahydrofuran 3.1: potassium tert-butylate / N,N-dimethyl-formamide / 20 °C 4.1: acetic anhydride; sodium carbonate / acetic acid / Reflux 4.2: Reflux 5.1: potassium carbonate / acetone / 24 h / 20 °C View Scheme
参考文献
Le, Tin Thanh; Chau, Nguyet Trang Thanh; Nguyen, Tai Tan; Brien, Josselin; Thai, Trieu Tien; Nourry, Arnaud; Castanet, Anne-Sophie; Nguyen, Kim Phi Phung; Mortier, Jacques
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 601 - 608
反应条件
water; potassium hydroxide Reflux;
参考文献
UNIVERSITE DU MAINE (LE MANS)
Patent: US2010/331398 A1, 2010 ;
Location in patent: Page/Page column 14 ;
反应条件
1.1: potassium hydroxide / water / Reflux 2.1: 2,2,6,6-tetramethylpiperidinyl-lithium / tetrahydrofuran / 0 - 20 °C 2.2: 2 h / 20 °C View Scheme
参考文献
Le, Tin Thanh; Chau, Nguyet Trang Thanh; Nguyen, Tai Tan; Brien, Josselin; Thai, Trieu Tien; Nourry, Arnaud; Castanet, Anne-Sophie; Nguyen, Kim Phi Phung; Mortier, Jacques
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 601 - 608
