(4-溴-2,6-二甲基苯基)硼酸合成路线 (共 1 条)
反应条件
1: 5-bromo-2-iodo-1,3-dimethyl-benzene With n-butyllithium in tetrahydrofuran; hexane T=-75 - -70°C; 0.5 h; 2: boric acid trimethyl ester in tetrahydrofuran; hexane T=-75 - 20°C; 3 h;
参考文献
SYNGENTA LIMITED; SYNGENTA PARTICIPATIONS AG
Patent: WO2009/74314 A1, 2009 ;
Location in patent: Page/Page column 169 ;