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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6-乙氧基-3-吡啶醇
合成路线
（共 11 条）
116178-33-7
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
in toluene T=45°C; 1 h;
参考文献
Kurita, Jyoji; Yoneda, Takeharu; Kakusawa, Naoki; Tsuchiya, Takashi
Heterocycles, 1987 , vol. 26, # 12 p. 3085 - 3088
4432-69-3
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: dimethylformamide 2: m-chloroperbenzoic acid (m0CPBA) 3: 100 percent / Al2O3 / diethyl ether; methanol 4: various solvent(s) / 1.5 h / 140 °C 5: CH2Cl2 6: 60 percent / benzene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
116178-12-2
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: m-chloroperbenzoic acid (m0CPBA) 2: 100 percent / Al2O3 / diethyl ether; methanol 3: various solvent(s) / 1.5 h / 140 °C 4: CH2Cl2 5: 60 percent / benzene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
116178-15-5
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: 100 percent / Al2O3 / diethyl ether; methanol 2: various solvent(s) / 1.5 h / 140 °C 3: CH2Cl2 4: 60 percent / benzene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
142-08-5
2-羟基吡啶
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: 54 percent / CH2Cl2 / 24 h / Ambient temperature 2: 42 percent / benzene / Irradiation 3: 95 percent / mCPBA / CH2Cl2 / 8 h / Ambient temperature 4: 72 percent / various solvent(s) / 150 °C 5: 47 percent / 0.5N aq. HCl / acetone / 4 h / Ambient temperature 6: 42 percent / 0.1N aq. NH3 / diethyl ether 7: CH2Cl2 / 3 h / ice-bath 8: 60 percent / toluene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
132433-20-6
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: 42 percent / benzene / Irradiation 2: 95 percent / mCPBA / CH2Cl2 / 8 h / Ambient temperature 3: 72 percent / various solvent(s) / 150 °C 4: 47 percent / 0.5N aq. HCl / acetone / 4 h / Ambient temperature 5: 42 percent / 0.1N aq. NH3 / diethyl ether 6: CH2Cl2 / 3 h / ice-bath 7: 60 percent / toluene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
132433-25-1
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: 95 percent / mCPBA / CH2Cl2 / 8 h / Ambient temperature 2: 72 percent / various solvent(s) / 150 °C 3: 47 percent / 0.5N aq. HCl / acetone / 4 h / Ambient temperature 4: 42 percent / 0.1N aq. NH3 / diethyl ether 5: CH2Cl2 / 3 h / ice-bath 6: 60 percent / toluene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
132433-52-4
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: 42 percent / 0.1N aq. NH3 / diethyl ether 2: CH2Cl2 / 3 h / ice-bath 3: 60 percent / toluene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
132433-40-0
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: 47 percent / 0.5N aq. HCl / acetone / 4 h / Ambient temperature 2: 42 percent / 0.1N aq. NH3 / diethyl ether 3: CH2Cl2 / 3 h / ice-bath 4: 60 percent / toluene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
132433-30-8
→
反应条件
116178-39-3
6-乙氧基-3-吡啶醇
反应条件
1: 72 percent / various solvent(s) / 150 °C 2: 47 percent / 0.5N aq. HCl / acetone / 4 h / Ambient temperature 3: 42 percent / 0.1N aq. NH3 / diethyl ether 4: CH2Cl2 / 3 h / ice-bath 5: 60 percent / toluene / 1 h / 45 °C View Scheme
参考文献
Kurita; Yoneda; Kakusawa; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 11 p. 2911 - 2918
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