[(2-氯乙氧基)甲基]膦酸二乙酯合成路线 （共 6 条）
反应条件
T=125°C; Arbuzov reaction;
参考文献
Wormstadt; Brinckmann; Gutschow; Eger
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 5 p. 1187 - 1191
反应条件
1: 99 percent / Dowex 50X8 (H(+)-form) / ethanol / 30 h / Heating 2: 50 percent / CCl4, triphenylphosphine / 4 h / Heating View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 52, # 11 p. 2801 - 2809
反应条件
tetrachloromethane; triphenylphosphine 4 h; Heating;
参考文献
Holy, Antonin; Rosenberg, Ivan
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 11 p. 2801 - 2809
反应条件
1) 90 min at 90 deg C 2) 4 h at 125 deg C; Yield given;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 54, # 8 p. 2190 - 2210
反应条件
sodium hydride in N,N-dimethyl-formamide T=80°C; 15 h;
参考文献
Holy, Antonin; Rosenberg, Ivan
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 11 p. 2801 - 2809
反应条件
1: 73 percent / dimethylformamide / 7 h / 120 °C 2: hydrazine / ethanol / 1 h / Heating 3: Et3N / ethanol / 20 h / Heating 4: 92 percent / 3 h / 120 °C 5: 87 percent / NH3 liquid / tetrahydrofuran; dimethylsulfoxide / 24 h / 25 °C View Scheme
参考文献
Dang, Qun; Liu, Yan; Erion, Mark D.
Nucleosides and Nucleotides, 1998 , vol. 17, # 8 p. 1445 - 1451
