1: 85 percent / hydrochloric acid / methanol; H2O / 0.5 h / Ambient temperature 2: 96 percent / Bu3SnH / AIBN / methanol; toluene / 1 h / Heating 3: 94 percent / sodium / methanol / 0.5 h / Ambient temperature 4: 82 percent / 6M-HCl / methanol; H2O / 24 h / Heating View Scheme
参考文献
Sammes, Peter G.; Thetford, Dean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 111 - 124
1: 85 percent / hydrochloric acid / methanol; H2O / 0.5 h / Ambient temperature 2: 96 percent / Bu3SnH / AIBN / methanol; toluene / 1 h / Heating 3: 94 percent / sodium / methanol / 0.5 h / Ambient temperature 4: 82 percent / 6M-HCl / methanol; H2O / 24 h / Heating View Scheme
参考文献
Sammes, Peter G.; Thetford, Dean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 111 - 124
1: 85 percent / hydrochloric acid / methanol; H2O / 0.5 h / Ambient temperature 2: 96 percent / Bu3SnH / AIBN / methanol; toluene / 1 h / Heating 3: 94 percent / sodium / methanol / 0.5 h / Ambient temperature 4: 82 percent / 6M-HCl / methanol; H2O / 24 h / Heating View Scheme
参考文献
Sammes, Peter G.; Thetford, Dean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 111 - 124
1: 85 percent / hydrochloric acid / methanol; H2O / 0.5 h / Ambient temperature
2: 96 percent / Bu3SnH / AIBN / methanol; toluene / 1 h / Heating
3: 94 percent / sodium / methanol / 0.5 h / Ambient temperature
4: 82 percent / 6M-HCl / methanol; H2O / 24 h / Heating
View Scheme
参考文献
Sammes, Peter G.; Thetford, Dean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 111 - 124
With hydrogenchloride in methanol; water 0.5 h; Ambient temperature;
参考文献
Sammes, Peter G.; Thetford, Dean Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 111 - 124