(5-氧代-5-苯基-戊基)-氨基甲酸叔丁酯合成路线 （共 7 条）
反应条件
1: in tetrahydrofuran T=-78°C; 0.666667 h; 2: With water in tetrahydrofuran
参考文献
Anderson, Kevin; Chen, Yi; Chen, Zhi; Luk, Kin-Chun; Rossman, Pamela Loreen; Sun, Hongmao; Wovkulich, Peter Michael
Patent: US2012/184542 A1, 2012 ;
Location in patent: Page/Page column 105 ;
US 20120184542 A1
反应条件
in tetrahydrofuran T=-70 - 20°C;
参考文献
Williams, Glynn D.; Pike, Richard A.; Wade, Charles E.; Wills, Martin
Organic Letters, 2003 , vol. 5, # 22 p. 4227 - 4230
反应条件
1: 90 percent / n-BuLi / CH2Cl2 / -78 - 20 °C 2: 43 percent / tetrahydrofuran / -70 - 20 °C View Scheme
参考文献
Organic Letters, , vol. 5, # 22 p. 4227 - 4230
反应条件
1: 90 percent / n-BuLi / CH2Cl2 / -78 - 20 °C 2: 43 percent / tetrahydrofuran / -70 - 20 °C View Scheme
参考文献
Organic Letters, , vol. 5, # 22 p. 4227 - 4230
反应条件
magnesium 1.) THF, 2.) -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 1 p. 228 - 234
反应条件
1: 92 percent / TFA / 2 h / 18 - 22 °C 2: 70 mg / NaBH4 / H2O; methanol / 18 - 22 °C View Scheme
参考文献
Williams, Glynn D.; Pike, Richard A.; Wade, Charles E.; Wills, Martin
Organic Letters, 2003 , vol. 5, # 22 p. 4227 - 4230
反应条件
trifluoroacetic acid
T=18 - 22°C; 2 h;
参考文献
Williams, Glynn D.; Pike, Richard A.; Wade, Charles E.; Wills, Martin
Organic Letters, 2003 , vol. 5, # 22 p. 4227 - 4230
