N-(2,2-二乙氧基乙基)-N’-甲氧基脲合成路线 (共 4 条)
反应条件
triethylamine in chloroform T=20°C; 0.75 h;
参考文献
Bock, Veronika; Kloetzer, Wilhelm; Singewald, Nicolas; Strieder, Georg
Synthesis, 1987 , # 12 p. 1058 - 1060
反应条件
1: 80 percent / hydrazine hydrate / 2.5 h / Heating 2: aq. HCl, NaNO2 / CHCl3 / 0.25 h / -5 °C 3: CHCl3 / Heating 4: 77 percent / (C2H5)3N / CHCl3 / 0.75 h / 20 °C View Scheme
参考文献
Bock, Veronika; Kloetzer, Wilhelm; Singewald, Nicolas; Strieder, Georg
Synthesis, 1987 , # 12 p. 1058 - 1060
反应条件
1: aq. HCl, NaNO2 / CHCl3 / 0.25 h / -5 °C 2: CHCl3 / Heating 3: 77 percent / (C2H5)3N / CHCl3 / 0.75 h / 20 °C View Scheme
参考文献
Bock, Veronika; Kloetzer, Wilhelm; Singewald, Nicolas; Strieder, Georg
Synthesis, 1987 , # 12 p. 1058 - 1060
反应条件
hydrogenchloride in ethanol T=20°C; 5 h;
参考文献
Synthesis, , # 12 p. 1058 - 1060