(E)-4’-羟基-3,4,5-三甲氧基二苯乙烯合成路线 （共 11 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 0.5 h; Ambient temperature;
参考文献
Cushman, Mark; Nagarathnam, Dhanapalan; Gopal, D.; Chakraborti, Asit K.; Lin, Chii M.; Hamel, Ernest
Journal of Medicinal Chemistry, 1991 , vol. 34, # 8 p. 2579 - 2588
反应条件
sodium hydroxide in tetrahydrofuran 2 h; Heating;
参考文献
Moro, Angelica Venturini; Cardoso, Flavio Sega P.; Correia, Carlos Roque D.
Tetrahedron Letters, 2008 , vol. 49, # 39 p. 5668 - 5671
反应条件
quinoline; copper T=200°C; 3 h; Inert atmosphere; diastereoselective reaction;
参考文献
Xiao, Chun-Fen; Zou, Yong; Du, Jian-Li; Sun, Hong-Yi; Liu, Xian-Ke
Synthetic Communications, 2012 , vol. 42, # 9 p. 1243 - 1258
反应条件
1: 27 percent / NaH / benzene / 16 h / Ambient temperature 2: 80 percent / n-Bu4NF / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 8 p. 2579 - 2588
反应条件
1: 27 percent / NaH / benzene / 16 h / Ambient temperature 2: 80 percent / n-Bu4NF / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 8 p. 2579 - 2588
反应条件
1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexanes / 0.33 h / -20 °C / Inert atmosphere 2.2: 3 h / -20 - 20 °C / Inert atmosphere 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.67 h / 20 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 6 p. 2586 - 2595
参考文献
Farmaco, Edizione Scientifica, , vol. 12, p. 380,385
反应条件
1: acetic anhydride; triethylamine / 140 °C 2: quinoline; copper / 220 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 19 p. 5898 - 5905
反应条件
1: acetic anhydride; triethylamine / 140 °C 2: quinoline; copper / 220 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 19 p. 5898 - 5905
反应条件
1: acetic anhydride; triethylamine / 6 h / 110 °C 2: quinoline; copper / 3 h / 200 °C / Inert atmosphere View Scheme
参考文献
Synthetic Communications, , vol. 42, # 9 p. 1243 - 1258
